Based upon these processes, a set of generalized design heuristics are presented in this work. These include:
The heuristics presented in this work will help engineers to determine the configuration, operational recipe, and control structure of semicontinuous processes in the conceptual design stages. Properties such as the order of the relative volatilities of the chemical species, the structure of the chemical reactions, the presence of azeotropes, etc., are the basis for these heuristics.
References
1. Phimister, J. R. and W. D. Seider, "Semicontinuous, middle-vessel distillation of ternary mixtures." AIChE J., 46, 8 (2000): pp. 1508-1520.
2. Adams II, T. A., and W. D. Seider, “Ethyl Lactate Production Using Semicontinuous Distillation with Reaction in an Auxiliary Vessel and Pervaporation,” 2007 AIChE Spring Nat'l. Meet., Houston, TX, Apr 23-27 2007.
3. Adams II, T. A., and W. D. Seider, “Semicontinuous Reactive Distillation for Specialty Chemical Production: Economic Comparison with Batch and Continuous Processing,” 2005 AIChE Fall Nat'l. Meet., Cincinnati, OH, Oct 30-Nov 2 2005; p 6251-6257. Plenary session.
4. Adams II, T. A., and W. D. Seider, “Semicontinuous Process Intensification: Combining Reactive Extraction, Reactive Distillation, And Binary Distillation For Production Of 1,3-Propanediol”, 2007 AIChE Annual Meet., Salt Lake City, UT, Nov 4-9, 2007.